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Stable Isotope Geochemistry

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Stable Isotope Geochemistry <[log in to unmask]>
Subject:
Reference Gas Peak Size Changes with Temp.
From:
"Brian M. Giebel" <[log in to unmask]>
Date:
Wed, 9 Nov 2005 12:20:01 -0500
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Stable Isotope Geochemistry <[log in to unmask]>
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Greetings,

I'm using GC-C-IRMS and I'm having a problem with my reference CO2.  The
reference gas is plumbed directly into the GC oven, flows through the
combustion furnace and nafion water scrubber, and finally to the mass
spec.

It seems that as my GC oven temperature increases, my reference gas peak
sizes decrease.  Has anyone witnessed this on their system?  Any
suggestions?

Cheers,

Brian




Brian M. Giebel
UM-RSMAS
Division of Marine & Atmospheric Chemistry
Office: 305-421-4724
Cell: 631-662-4931
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NEW OFFICE TELEPHONE EXCHANGE 305-421-4724
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