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Stable Isotope Geochemistry

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Subject:
Re: Condensation of sample water on septum
From:
Gerard Olack <[log in to unmask]>
Reply To:
Stable Isotope Geochemistry <[log in to unmask]>
Date:
Wed, 14 Dec 2005 10:26:39 -0500
Content-Type:
text/plain
Parts/Attachments:
text/plain (33 lines)
Hi Magda & Diana--

After equilibration, we've taken to removing taking the tubes out (two 
at a time) and tapping the sides of the cap to move the condensate to 
one side, then shaking it down.  There isn't much of a problem with the 
runs afterwards.  Alternatively, you may consider putting a blanket on 
top of the gasbench while it's equilibrating to see if that cuts down on 
condensation.

take care

gerry

Diana Bojic wrote:

> Dear All,
> We are new in mass spectrometry "business" but we already have 
> problems. We are trying to do water equilibration on gas bench II and 
> delta +XP. We have problem with evaporation of sample water in vials. 
> Water is condensing on the septum and when  the needle penetrate in 
> septum small amount if water is  entering the system.  We have heard 
> for building a cooler but we are interesting in otherer possibilities. 
> Does anybody have some suggestions? 
>
>  
>
> Thanks
>
>  
>
> Magda & Diana
>

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