Skip Navigational Links
LISTSERV email list manager
LISTSERV - LIST.UVM.EDU
LISTSERV Menu
Log In
Log In
LISTSERV 17.5 Help - ISOGEOCHEM Archives
LISTSERV Archives
LISTSERV Archives
Search Archives
Search Archives
Register
Register
Log In
Log In

ISOGEOCHEM Archives

Stable Isotope Geochemistry

ISOGEOCHEM@LIST.UVM.EDU

Menu
LISTSERV Archives LISTSERV Archives
ISOGEOCHEM Home ISOGEOCHEM Home

Log In Log In
Register Register

Subscribe or Unsubscribe Subscribe or Unsubscribe

Search Archives Search Archives
Options: Use Forum View

Use Monospaced Font
Show Text Part by Default
Show All Mail Headers

Message: [<< First] [< Prev] [Next >] [Last >>]
Topic: [<< First] [< Prev] [Next >] [Last >>]
Author: [<< First] [< Prev] [Next >] [Last >>]

Print Reply
Subject:
vacuum problem on Delta Plus
From:
Bernie Genna <[log in to unmask]>
Reply To:
Stable Isotope Geochemistry <[log in to unmask]>
Date:
Thu, 4 Aug 2005 12:54:07 -0400
Content-Type:
text/plain
Parts/Attachments:
text/plain (24 lines)
Hi All,

      We have a Delta Plus XL Mass Spectrometer that we vented last week to 
replace one of the quartz spacers in the source. While all the parts we 
laid on the table overnight (we had to order the spacer), the cooling unit 
in our building failed and the lab temp got up to 85 degrees. We had 
inadvertently left our cooling water turned after venting the instrument. 
When we reassembled the source and tried to pump down, the source vacuum 
will only pump down to 5X10-5. Thermo said that the source flange clamps 
were overtightened and the knife edge seal that seals the source housing 
needed to be replaced. Well we finally got the source flange clamps (from a 
secondary source), and replaced the knife edge seal and see that the source 
vacuum is still 10-5. The forevac vacuum is normal (2X10-3). My 
question(s): Could the temperature difference between the cooling water (15 
degrees) and the air temperature (85 degrees) cause problems in the vented 
source housing and/or exposed flight tube?  Could the high vacuum gauge be 
faulty? Do I suddenly not know how to tighten a source gasket to get the 
proper vacuum?

Any ideas will be very much appreciated.

Bernie Genna
NCSU

ATOM RSS1 RSS2

LIST.UVM.EDU CataList Email List Search Powered by LISTSERV