Subject: | |
From: | |
Reply To: | |
Date: | Tue, 26 Feb 2008 15:14:57 -0500 |
Content-Type: | text/plain |
Parts/Attachments: |
|
|
Hi there,
I am still puzzled about he delayed peak retention time and elevated N2
baseline. Neither a large leak or blockage (which should cause the observed
effects) is detectable, at least not in the components that I can test directly
or indirectly by bypassing them (autosamples, combustion / reduction column,
water trap, GC column, TCE detector, O2 loops, Conflo III).
While I am still searching for a solution, I would like to describe two more
things that I haven't mentioned before. First, the flash combustion is delayed
by about 10 sec.. Second, when I take out the He-diluter, the N2 baseline
jumps up immidiately from 6 to 12 mV but then slowly creeps up to about 30
to 40 mV over the duration of 200 seconds. I am not sure if these time lags
are related to the original problem but maybe it rings a bell for someone...?
Thanks, Bjoern
|
|
|