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Stable Isotope Geochemistry

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Subject:
From:
"Willi A. Brand" <[log in to unmask]>
Reply To:
Stable Isotope Geochemistry <[log in to unmask]>
Date:
Thu, 1 Dec 2005 15:47:40 +0100
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Hi,
we are operating a number of D+XL's since long and seem to have been 
lucky with the HV tripping business. So, I can offer only a suspicion as 
to where to look for. I have 3 suggestions:
1. If the ion source has been operated for some time (with high 
sensitivity, i.e. high ion currents a week may be plenty) there is a 
risk that enough material has been sputtered from the entrance slit area 
that the insulation across the big quartz ring has deteriorated enough 
to cause some sparking. Cleaning then is necessary (with HCl to get rid 
of Ta, with HCl+HNO3 in the case of a Au slit)
2. All HV supplies have a maximum load setting in order to save peoples 
lives. In order to accomplish this task, the trip circuits also have to 
be fast. However, if they are too fast, they may become vulnerable 
against minor sparks as mentioned under (1). In the D+XL one can at 
least set the trip level on the PCB (R33, 'overload adjust'), it might 
be set too sensitive. Clockwise is less sensitive (I think). The 
standard setting is arount '1 pm'. A word of caution: Do NOT operate on 
the source supply with the HV on !!
3. The ion source is protected against high pressures using the Penning 
gauge. If the Penning starts to deliver erroneous pressures, the trip 
might be initiated. However, this should trip the whole ion source, not 
just the HV.

I am not so familiar with the new electronics in the D+XP, but the 
design principles should be similar.

Willi

-- 
.....................................................................

Willi A. Brand, Stable Isotope Laboratory      [log in to unmask]

Max-Planck-Institute for Biogeochemistry

Beutenberg Campus
Hans-Knoell-Str. 10, 07745 Jena, Germany      Tel: +49-3641-576400
P.O.Box 100164,      07701 Jena, Germany      Fax: +49-3641-577400

    	http://www.bgc-jena.mpg.de/
   	http://www.bgc-jena.mpg.de/service/iso_gas_lab/

GASIR 2005 in Jena:
http://www.bgc-jena.mpg.de/service/iso_gas_lab/gasir2005/index.shtml


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