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| Date: |
Thu, 26 Apr 2001 16:22:40 +0200 |
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7bit |
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| Organization: |
Institute of Soil Science, University of Bayreuth,
D-95440 Bayreuth, Germany |
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Dear List members,
most recently, we are observing an instability of our Delta plus IRMS
coupled with a Trace GC 2000 and a combustion interface III. If we run
standard on/off with a constant CO2 amount we get pretty constant d13C
values. However, if we try to vary the CO2 pressure there is a drift of
up to 2 delta per mil. If we switch over to EA-IRMS, the drift
disappears.
What is a bit strange are increasing delta vs SMOV 18/16 values with
time injecting the same samples although the 45/44 and the d17O corr
d13/12 ratios remained more or less constant over time.
Any suggestions are highly appreciated.
Kind regards
Bruno
Dr. Bruno Glaser
Insitute of Soil Science and Soil Geography
University of Bayreuth
D-95440 Bayreuth
Germany
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