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Stable Isotope Geochemistry

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Subject:
Re: C/O isotopes from organic rich carbonates
From:
[log in to unmask] (Stephen S. Howe)
Date:
Fri, 21 Jun 1996 08:17:15 -0500
Content-Type:
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Stefan:

Presently, we roast lacustrine and marine sediments and soils in a tube
furnace at 350°C under vacuum to remove organic matter that might present
problems during Isocarb runs.  In the past, I have used hydrogen peroxide
with no problems on foraminifera.

Steve


>Dear isogeochemist
>I'd like to bring up a question presented by Valderez Pinto Ferreira a
>month ago.
>We have to analyze some "exotic" carbonate samples from a drain-trench for
>C and O isotopes. Unfortunately, the material is contaminated by strongly
>smelling "organics". As we donot want to ruin (?) our masspec and we donot
>own a plasma oven our questions are:
>is there an easy way to get rid of the contamination?
>Has there agreement been settled about the effects of H2O2 treatment?
>Are there newer references than that of Charef & Sheppard (1984) or any
>personal experiences?
>
>Any help will be highly apreciated,
>greetings
>Stefan


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Stephen S. Howe                  Office:  (847) 491-8180
Northwestern University          Stable Isotope Lab:  (847) 491-8182
Dept. of Geological Sciences     Geochemistry Lab:  (847) 491-8184
1847 Sheridan Road               FAX:  (847) 491-8060
Evanston, IL  60208-2150         e-mail:  [log in to unmask]
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