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| Date: | Wed, 21 Nov 2001 16:58:12 -0500 |
| Content-Type: | text/plain |
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Dear Graeme
I think the plastic bottles are OK for the short time storage. we regular
do 13C and 14C analyses and most samples come in plastic Nalgen bottles. I
have some experience with brines, they are horrible.
I found that the best way to clean that kind of samples from S compounds is
purification of CO2 after extraction from solution. I collected gas in the
tube with Cu, CuO and Ag sealed them of and heated for 2-3 hours under t=525C.
That method works fine and we did not have a problem with graphitization
after this purification.
Alex Cherkinsky
Dr.Alexander Cherkinsky
Geochron laboratories,
Radiocarbon Lab Manager
711 Concord Ave.
Cambridge, MA 02138, USA
Phone: 617 876-3691
Fax: 617 661-0148
E-mail:[log in to unmask]
At 10:57 AM 11/21/01 +1300, you wrote:
Are plastic (PVC) bottles adequate for short term (days) storage of
groundwaters
before extraction of C for 13C and 14C analysis?
What is the best way to treat for sulfur in the oilfield brines before
extracting the CO2 ?
Graeme Lyon
Dr G L Lyon,
Rafter Building,
Institute of Geological & Nuclear Sciences Ltd,
P O Box 31 312, [courier address: 30 Gracefield Road]
Lower Hutt,
New Zealand
Phone: 64 + 4 + 570 4637
Fax : 64 + 4 + 570 4657
Email: [log in to unmask]
Web : www.gns.cri.nz
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