Stable Isotope Geochemistry


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Sender: Stable Isotope Geochemistry <[log in to unmask]>
From: Benjamin Uveges <[log in to unmask]>
Date: Fri, 30 Oct 2020 19:13:08 +0000
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Hello Isogeochem,

We have an older Delta plusXP IRMS that we got working again last Fall. We recently had some issues with our EA system so we closed the Delta off from the Conflo, and it has been sitting for a little over 2 weeks while we wait for parts to fix the EA.

Yesterday I noticed that the Box and Trap currents were fluctuating quite a bit. So, I ran a box/trap current scan to see what they were doing through time, and found that they were each jumping between ~0.75 and 0.55 mA about 16 times a second. I have seen drift in these currents before as filaments age, but never such large, rapid oscillations. Everything else seems to be stable, and the vacuum is also fine. Prior to this, Box and Trap were stable at about 0.65 and 0.75 mA.

Has anyone else experienced this? Is this just a sign that the filament is about to go, or that the source needs to be cleaned? Or possibly something more serious? Just trying to get a better idea of what we are up against before we vent it and pull the temperamental source block out.

Any insight would be greatly appreciated. Thanks!

Benjamin Uveges, PhD.
Postdoctoral Associate
Department of Earth, Atmospheric and Planetary Sciences | Massachusetts Institute of Technology | E25-637: 45 Carleton Street | Cambridge, MA 02142.