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Stable Isotope Geochemistry

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Stable Isotope Geochemistry <[log in to unmask]>
Subject:
Multiprep dD of water
From:
Jason Curtis <[log in to unmask]>
Date:
Wed, 9 May 2001 16:50:59 -0400
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Stable Isotope Geochemistry <[log in to unmask]>
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Hi,
        Can anyone provide me with basic methodology for running dD of
water using a MultiPrep (either Micromass or Matt Emmons version).  We
routinely run d18O of water but have yet to try dD.

Do you use Pt-Al catalyst? Hokka beads? Glass rods?
Do you use the auto hydrogen injection?  A glove bag?
What temperature for multiprep?  Equilibration times?

Thanks in advance for any info.  Jason

_______________________________________________________________________________
Jason Curtis, Ph.D.
Stable isotope mass spec lab manager
Assistant-In Geochemistry, Department of Geological Sciences
241 Williamson Hall, PO Box 112120
University of Florida, Gainesville FL 32611
phone 352-392-2296, lab 352-392-3344, fax 352-392-9294, e-mail [log in to unmask]

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