Hi, Paul: Charcoal made in SKC Inc. is sealed in a glass tube. One tube is enough to treat about 4ml of water. It is very convenient and effective. The address is: 334 Valley View Road, Eighty Four, Pennsylvania 15330. Good luck. Dachun Zhang Isotope Lab ZymaX Paul Brooks wrote: > First I would like to thank all of you who replied on the storage of IAEA > standards. The information was very useful. > > We are using FM Gas Bench for 18O equilibrations with 0.2% CO2 in > Helium. This method usually works very well. Unfortunately we have a > batch of water extracted from grass leaves that report results that make no > sense. It appears that some of them actually generated CO2, while other > took it out of the atmosphere! Running them twice made no difference and > yet other samples and standards in the run analyzed very well. > > It has been suggested that this is probably due to contamination from > organic volatiles in the sample, and that we should add some activated > charcoal to each sample, shake them and then re-equilibrate them. I am not > familiar with this method. Has anyone else ever used this and do they have > a reference and suggestions as to the type of carbon? > > Thanks in advance, > > Paul. > > Paul D. Brooks, > Dept. ESPM-ES, > 147 Higard Hall MC 3110, > UC Berkeley, Ca. 94720-3110. > > phone (510)643-1748, > FAX (510)643-5098.