We have used 1/8" valco valves under vacuum and pressure and had no problems as long as you have the appropriate ferrules. Also, we recommmend type M rotor material (the material inside the valve responsible for sealing among ports) as the type P valve greatly influences 13C and 18O in CO2 samples. andy --- Michael Bock <[log in to unmask]> wrote: > Dear all, > > I go about building a preconcentration system for methane in small air > samples. > Did anyone use Valco switching valves (6port, 1/8 or 1/4'', type 6UWE or > 6MWE2) under vacuum conditions? > What leak rate did you observe at which pressures? Any recommendations > concerning the switching between vacuum conditions in one postion and > non-vacuum in the other? > > Any infomation will be very much appreciated... > > Regards > Michael > > -- > Michael Bock > Alfred Wegener Institute for Polar and Marine Research > Am Alten Hafen 26 > 27568 Bremerhaven > Germany > tel: +49-471-4831-1967 > lab: +49-471-4831-1026 > fax: +49-471-4831-1926 > email: [log in to unmask] > Andrew Schauer Stable Isotope Ratio Facility for Environmental Research Department of Biology University of Utah 257 S. 1400 E. Salt Lake City,UT 84112 USA [log in to unmask] 801.581.8917