>Hi Jason, > >I also had to source a supply of the PCTFE disks and silicone rubber >septa after realizing that the only reasonable option is make them yourself. > >I use the same PCTFE sheets that Kim described but I also buy rolls >of 1/8" red silicone rubber which I cut into 12" x 12" sheets. I lay >the PCTFE onto a sheet of rubber, stack up ~20 sheets and take them >to an company here in Calgary that specializes in rubber and septa >and stuff and they punch them out together (~300 per sheet). When I >get them back the PCTFE disks and rubber septa are often loosely >stacked together, making it slightly easier to stuff them into the caps. > >It takes a bit of testing to get the exact die-punch needed for your >vial (something the company did for me) but the cost per cap is now >at least in the reasonable price range ~$CND 0.60. > >Cheers, >Steve > >At 11:12 AM 4/13/2007, you wrote: >>Hi All, >> I am rapidly running out of septa for my Multiprep vials >> and need to find a new supplier. Typically I only use the >> Multiprep for oxygen isotopic analysis of waters. I have only >> used red rubber septa with kel-f disks that I got from Matt Emmons >> of Mountain Mass Spec. Matt seems to be out of the business as he >> does not answer calls or emails. >>So I need a new source. >> >>I need these for Wheaton vials (wheaton number 986284, 1 ml, >>13mmX44mm, screw cap size 13-425), not exetainers. >> >>I have made my own using a 12mm arch punch and 0.125 inch (3mm) >>material but would rather just be able to buy them. Does anyone >>have a source of this type of septa? >> >>If I have to go the complete custom route does anyone have >>suggestion as to septa material (silicone, butyl, red rubber, >>viton) and inert disk (PTFE) or not? Does the advice change any >>for hydrogen isotopes on water? >> >>Thanks in advance for any advice. Jason >> >>Jason Curtis, Ph.D. >>Stable Isotope Mass Spec Lab manager >>Associate-In Geochemistry >>Department of Geological Sciences >>241 Williamson Hall >>University of Florida >>Gainesville, FL 32611 >>[log in to unmask], office 352-392-2296 >>lab 352-392-3344, fax 352-392-9294 > >Stephen Taylor >Lab Manager, Isotope Science Lab, >University of Calgary, Physics & Astronomy, >2500 University Dr. N.W. >Calgary, Alberta, >Canada, T2N 1N4 >(p) 403 220 8268 >(f) 403 220 7773 >[log in to unmask] >www.phas.ucalgary.ca/isl