Matheus We also tried it with little success. However, Dissolved HCO3, CO2, and CO3 concentrations are easy to measure by acid/base titration. Any of the general geochemistry books (Drever, Stumm & Morgan, Langmuir etc) have the methodology. We use a digital titrator and pre-packed reagents from by Hach (worldwide suppliers of this type of kit) which is very easy to use and do our DIC measurements in the field. Ian ______________________________________________ Dr Ian Cartwright Head - School of Geosciences Hydrogeology and Stable Isotopes Monash University Clayton Vic. 3800, Australia t: 03 9905-4887 / 4879, f: 03 9905-4903 ...water, our greatest resource