Dear Karen and isotopers, As an alternative method to heavy liquid separation, this paper (see below) describes a magnetic separation method. Quartz+feldspar mixtures are treated with HF, the feldspar is etched, quartz remains intact, then the sample is mixed with magnetite powder. The magnetite grains are stuck onto the rough surface of the feldspar and thus it could be magnetically separated from quartz. The questions might be: is there an effect on the d18O of the feldspar? can the magnetite be removed perfectly after the separation? I think it might be worth trying. Iacumin, P and Quercioli, C. (1993): A new technique for quantitative separation of quartz from feldspars. Eur. J. Mineral., 5, 677-678. Cheers, Attila Dr. Attila Demeny Laboratory for Geochemical Research Hungarian Academy of Sciences Budapest, Budaorsi ut 45, H-1112, Hungary tel/fax: 36-1-319-3145 e-mail: [log in to unmask]