Graham, you may wish to have a look at some of the fundamental papers of Nick Pingitore Jr. I analyzed stable isotopes and trace element contents of mixed aragonite-calcite samples from a sulfur deposit. At least in HCl leachates, trace baryte was likely dissolved in a few samples. Weaker acids are necessary to look for lattice bond barium in carbonates. Good luck Michael ****************************************************************** Dr. Michael E. Boettcher Biogeochemistry Max-Planck-Institute for Marine Microbiology Celsiusstr.1 D-28359 Bremen FRG