Hi Ben and Stefan,

i´m very grateful for your advices.

I wish you nice weekend and kind regards

Paul Hawelitschek

Leibniz Institute for Freshwater Ecology and Inland Fisheries (IGB)
Department of Chemical Analytics and Biogeochemistry
Müggelseedamm 301
12587 Berlin

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-----Ursprüngliche Nachricht-----
Von: Stefan Merseburger <[log in to unmask]>
Gesendet: Donnerstag 29 Oktober 2020 17:22
An: [log in to unmask]
Betreff: Re: [ISOGEOCHEM] Pyrolyses silver capsul fall over crucible

Hello Paul,

in addition to Bens comment. You could check with a level that your EA 
stands fully perpendicular. An other option is to use graphite crucibles 
that have a larger inner diameter -- if possible. The maximum I found is 
a octagonal one with a inner diameter of 5.2 mm in a 7 mm reactor 
( part n.: g52109.001e).

Kind regards,

Am 28.10.2020 um 16:38 schrieb Harlow, Benjamin:
> ule to land on the top of the crucible an


Stefan Merseburger
Tel.: +49 721 608-41678
Karlsruher Institut für Technologie
Institut für Geographie und Geoökologie
Reinhard-Baumeister-Platz 1
76131 Karlsruhe